Prof. Brent Fultz

Professor of Materials Science

Brent Fultz received his Ph.D. from U. C. Berkeley in 1982. He was a Presidential Young Investigator; he also received an IBM Faculty Development Award and a Jacob Wallenberg Scholarship. He has consulted for the electronics testing company, Everett Charles Technologies, and the Defense Science Board. Fultz authored or co-authored well over 150 refereed publications, edited four books, and with J. Howe is completing a graduate-level textbook on diffraction and microscopy of materials. Fultz's description of his research interests is:

1. The main thrust of my work from 1987-92 was to use modern ideas in kinetics to understand atom movements in crystalline alloys. There were three accomplishments:

  • Possibilities for controlling kinetic paths of alloys were demonstrated analytically, by Monte Carlo simulations, and by experiment.
  • We studied specific cases where kinetically-favored states are not expected from a free energy surface.
  • In alloys far from thermodynamic equilibrium, I found that saddle points in the free energy function cause ‘pseudostable states’ to occur in materials.
    I am not presently working on theoretical or experimental problems of the kinetics of atom movements, but I expect to return to this field in the future.
    B. Fultz, C. C. Ahn, S. Spooner, L. B. Hong, J. Eckert and W. L. Johnson, "Incipient Chemical Instabilities of Nanophase Fe-Cu Alloys Prepared by Mechanical Alloying", Metall. and Mater. Trans. A 27 (1996) 2934-2946.
    L. B. Hong and B. Fultz, "Phase diagrams of bcc alloys at low temperatures with ballistic atom movements", Phys. Rev. B 52 (1995) 6230-6237.

    2. By calorimetry experiments we showed that vibrational entropy is important for the thermodynamics of alloy phase stability. Vibrational entropy is new to the materials science community, and its importance was unexpected. We have begun to measure phonon spectra of materials by inelastic neutron scattering. From phonon spectra we learning why there are differences in vibrational entropy between different alloy phases. This work is performed at national laboratory facilities for neutron beam experiments such as the reactor at Oak Ridge (HFIR) and the spallation sources at Argonne (IPNS) and Los Alamos (LANSCE). For many other types of materials, we are trying to determine how differences in crystal structure or microstructure affect the vibrational entropy.
    L. J. Nagel, B. Fultz, and J. L. Robertson, "Vibrational Entropies of Phases of Co3V Measured by Inelastic Neutron Scattering and Cryogenic Calorimetry", Philos. Mag. B 75 (1997) 681-699.
    L. J. Nagel, B. Fultz, J. L. Robertson, and S. Spooner, "Vibrational entropy and microstructural effects on the thermodynamics of partially-disordered and ordered Ni3V", Phys. Rev. B, 55 (1997) 2903-2911.

    3. We are pursuing two new Mossbauer-type experiments. They are:
    i) diffraction from 57Fe atoms in specific chemical environments, and
    ii) inelastic scattering to measure the vibrational spectra of 57Fe atoms.
    Mossbauer diffraction is an unexplored technique that has a capability of combining spectroscopy with diffraction in ways not avialable to the three diffraction methods of x-ray, electron, and neutron diffraction. It can provide information to permit new studies on topic 1 above. The inelastic scattering methods are performed at the Advanced Photon Source at Argonne National Laboratory, and provide information useful for topics 2 and 4.
    i.) T. A. Stephens and B. Fultz, "Chemical environment selectivity in Mossbauer diffraction from 57Fe3Al", Phys. Rev. Lett. 78 (1997) p. 366-369.
    ii.) B. Fultz, C. C. Ahn, E. E. Alp, W. Sturhahn, T. S. Toellner, "Phonons in nanocrystalline 57Fe", Phys. Rev. Lett., in press.

    4. We began our work on nanocrystalline materials by determining the widths of their grain boundaries. We later tested two metallurgical design strategies for stabilizing nanocrystalline materials against growth of their crystallites. In a related problem, we have shown both by experiment and by Monte Carlo simulations that two-phase steady-states in driven alloys are caused by heterogeneities in the enthalpy density. Recently we have been measuring the vibrational spectrum of nanocrystalline materials, which are significantly different from materials having conventional crystallites. We are also studying the interaction of microwave radiation with nanocrystals.
    H. N. Frase, L. J. Nagel, J. L. Robertson, and B. Fultz, "Vibrational Density of States in Nanocrystalline Ni3Fe", Philos. Mag. B 75 (1997) 335.

    5. We have been studying electrochemical properties of metal hydrides for several years. This is a response to a technological need to improve the lifetime of nickel - metal hydride batteries. The work includes an alloy design philosophy based on the kinetic control of atom movements, for which some concepts of topic 1 above are useful. We have begun to develop lithium alloys for electrodes in rechargeable batteries.
    C. Witham, B. V. Ratnakumar, R. C. Bowman, Jr., A. Hightower, and B. Fultz, "Electrochemical Evaluation of LaNi5-xGex Metal Hydride Alloys", J. Electrochem. Soc., 143 (1996) L205-L208.

    6. We have just begun to study Tb-Dy alloys with giant magnetostriction (these materials change their length by about 1% in a modest magnetic field). Our intent is to design polycrystalline materials that exhibit much of the performance of single crystals.

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